Rouge de Ruthene, Ru 2 (OH) 2 C1 4 (NH 4) 7, is obtained from ammonia and ruthenium sesquichloride at 40° C., the product being purified by crystallization from ammonia.
The amorphous form readily slakes with water, and the aqueous solution yields a crystalline hydrated hydroxide approximating in composition to Sr(OH) 2.8H 2 O or Sr(OH) 2.9H 2 O, which on standing in vacuo loses some of its water of crystallization, leaving the monohydrated hydroxide, Sr(OH) 2 H 2 O
The heat at which the syrup boils in the clarifiers, 220° F., has the property of separating a great deal of the gum still remaining in it, and thus cleansing the solution of sugar and water for crystallization in the vacuum pans; and if after skimming the syrup is run into separators or subsider
When heated they liquefy; and if the heating be continued, the water of crystallization is driven off, the salt froths and^swells, and at last an amorphous powder remains.
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